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Attempts to reduce TaCl 5 with KC 8 or LiBH 4 in the presence of lithium diphenylformamidinato (LiDPhF) or potassium pyridinethiolato (Kpyt) are described. At low temperature the reaction of TaCl 5 , KC 8 and LiDPhF yields the mononuclear eight-coordinated compound Ta(DPhF) 4 2 which was found to be isostructural with the niobium analog 1. At room...
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