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Partial hydrolysis (H2O/Ln molar ratio=¼) of lanthanum di-iso-propylcarbamato complex, [La(O2CNiPr2)3], 1, afforded the tetranuclear μ-oxo derivative [La4O(O2CNiPr2)10], 2, which was structurally characterized by single crystal X-ray diffraction studies. The carbonato–carbamato derivative of lanthanum, [La4(CO3)(O2CNBu2)10], 3, was prepared by extraction of lanthanum ions from aqueous solution into...
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