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Reaction of [MoOCl5]2− with in situ generated H2Se under hydrothermal conditions (4M HCl, 140 °C) leads to reduction of Mo(V) to Mo(IV) with the formation of a triangular cluster Mo3(μ3-Se)(μ-O) 34+ in high yield. It is present in HCl solutions as aqua chlorocomplex [Mo3(μ3-Se)(μ-O)3(H2O)6Cl3]+ which was isolated and structurally characterized as supramolecular adduct with cucurbit[6]uril (CB[6]),...
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