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Polymer architecture can have a significant effect on the properties and potential applications of materials. In this study, arborescent polyisobutylene (PIB)‐poly(ethylene oxide) (PEO) graft copolymers with varying PEO content were synthesized from arborescent PIB‐co‐polyisoprene and compared with linear PIB‐PEO graft copolymers. By AFM imaging, phase separation was detected in a 48 wt% PEO arborescent...
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