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The reaction of FeCl 2 (HDPhF) 2 (HDPhF = N,N -diphenylformamidine) with methyllithium in Et 2 O followed by extraction into solvent mixtures containing THF, toluene and hexanes produces crystals of Fe 2 (μ-DPhF) 4 (I). This dinuclear compound contains four formamidinato bridges but in an arrangement that is highly distorted compared to the known paddle-wheel...
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