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In order to determine the role of the sulfur donors around the Co(III) site of the enzyme nitrile hydratase, we have synthesized a designed ligand PyPSMeH 2 (Hs are dissociable carboxamide hydrogens) with carboxamido nitrogens and thioether sulfur donors. Although Co(III) complexes with bound thioether groups have previously been synthesized with other ligands, attempts to synthesize such...
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