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Highly uniform and monodispersed CuCo2S4 ball‐in‐ball hollow nanospheres (HNSs) are successfully synthesized from CuCo‐glycerate nanospheres (NSs) precursors via a facile two‐step solvothermal process. The most influential parameter in anion exchange reaction between glycerate and sulfur ion is the solvothermal time, which plays a significant role in enhancing the structural and electrochemical properties...
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