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The use of acetylated phenyl 1-seleno-β-d-galactofuranoside as a glycosyl donor for the synthesis of protected d-Galf-β-(1 → 3)-α-d-Manp as its methyl or ethylthio glycoside has been demonstrated. Activation of the selenoglycoside over a thioglycoside acceptor by NIS/TfOH is extremely selective and gives the ethylthio disaccharide in 91% yield. The parent disaccharide is found as a terminal and...
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