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Single crystals of FePb4Sb6Se14, were obtained from solid‐state combination of high purity elemental powders at 873K for three days. Single crystal X‐ray structure determination revealed that the compound crystallizes in the monoclinic space group P21/c (no. 14) and adopts the structure of Jamesonite (FePb4Sb6S14). The structure contains two crystallographically independent lead atoms with monocapped...
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