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A single phase of MnSb2Se4 was synthesized by combining high‐purity elements at 773 K. Single‐crystal X‐ray diffraction revealed that MnSb2Se4 is isostructural with FeSb2Se4 crystallizing in the monoclinic space group C2/m with a = 13.076(3) Å, b = 3.965(2) Å, c = 15.236(4) Å, β = 115.1(2)°, Z = 4. MnSb2Se4 melts congruently at 790 K and is thermally stable up to 1000 K. Electronic band structure...
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