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3D morphology of poly(3‐hydroxybutyrate) (PHB), crystallized in the presence of diluents of poly(1,3‐trimethylene adipate) and poly(ethylene oxide), is probed using a novel approach coupled with selective etching. For interpreting the mechanisms of crystal periodic aggregation, various microscopic techniques and synchrotron microbeam X‐ray analysis are used to observe the top surface in connection...
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