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High operation temperatures and slow reaction kinetics are major obstacles to use MgH2 as a solid hydrogen store. We report here the synthesis of Nb2O5 hollow spheres (o‐Nb2O5) with wall thickness of approximately 50 nm and mossy surfaces using a facile hydrothermal and calcination process, which showed high activity in catalysis of MgH2 for hydrogen storage. The dehydrogenation onset temperature...
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