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A new ternary Metal–N–H sample of Mg–Ca–N–H has been prepared by mechanical ball milling—Mg(NH 2 ) 2 and CaH 2 (1:1) in a planetary ball mill machine. The structure and hydrogen desorption properties were investigated. The results show that pure H 2 gas can be released during ball milling. After 72h ball milling, ∼3.8H atoms (∼3.88wt%) were found to be detached from...
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