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A neat electroactive freestanding non‐woven mat was first prepared from poly(o‐methoxyaniline) (POMA) using an electrospinning technique without blending or grafting. Results showed that a continuous fibre structure was obtained for high weight‐average molecular weight M̄w of POMA, i.e. POMA forced to become more soluble when synthesized in the presence of CaCl2 and an alkoxyl‐ring‐substituted structure...
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