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A series of samples with the initial formula Mo3–xFexSb7 and Mo3–xNixSb7 have been prepared by solid state reaction at 873K, starting from the elements in the stoichiometric ratios. The materials were compressed via hot-pressing, and their thermoelectric properties determined. Single crystal data show that Ni atoms in part occupy the cubic voids of the Mo3Sb7 structure, as well as replace some Mo...
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