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Homogeneous titania–silica binary hydrogels were molded into various shapes, microhoneycomb, self-standing bundle, microfibers, and powder, by a unidirectional freezing method. Moreover, by freeze-drying the unidirectionally frozen samples, the honeycomb walls or microfibers obtained were converted into mesoporous cryogels which possessed considerable high surface areas (up to 1057m 2 g ...
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