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The ZnS nanoparticles were exclusively synthesized in the pores of the mesoporous silica (MS) particles which had been coated with two bilayers of poly(allylamine hydrochloride) (PAH)/poly(styrene sulfonate) (PSS) via the layer-by-layer (LbL) self-assembly technique. Measurements and analysis of XRD and TEM showed that the ZnS nanocrystals were inserted into the pores of the MS spheres. This approach...
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