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Highly transparent glass ceramics, synthesized from a glass precursor with a nominal composition of SiO2/ZnO/Ga2O3/Na2O/Cr2O3 (65:17:23:5:0.125), were prepared by glass crystallization. This method enables the synthesis of up to 50 wt.‐% of size‐controllable Cr3+‐doped ZnGa2O4 nanocrystals embedded in an SiO2‐rich glass matrix after crystallization at 900–1000 °C for 10 min. Rietveld refinements and...
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