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Monodispersed hollow ZnS microspheres have been successfully synthesized by a facile ethylenediamine tetraacetic acid (EDTA) mediated hydrothermal route. The sizes of the hollow spheres vary from 1.5 to 3.5 μm when the reaction temperature varied from 130 to 230 °C. The formation of these hollow spheres is attributed to the oriented aggregation of ZnS nanocrystals around the gas–liquid interface between...
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