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Hexagonal crystalline ultrathin ReSe2 flakes are synthesized for the first time by a chemical vapor deposition (CVD) method. The as‐synthesized ReSe2 flake is revealed as a novel structure, which has mirror‐symmetric single‐crystal domains inside, by polarization incident Raman and HRTEM. The successful development of the CVD method will facilitate research on the novel anisotropic electronic/optoelectronic...
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