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The photophysical properties of a few Ir(III) and Rh(III) complexes have been attempted to be correlated (1–4) with their 1O2 generation efficiencies. A very weakly emissive pyrene‐functionalized Ir(III) complex (1) produces 1O2 more efficiently than the other more emissive Ir(III) complexes. All of them have excited triplet state lifetimes (τT) in the microsecond regime. However, the pyrene‐functionalized...
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