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We report direct evidence for quintuplet spin states in a particular kind of reduced TiO2 anatase obtained by the mild oxidation of TiB2 under hydrothermal conditions. Continuous‐wave and pulse EPR spectroscopy at X and Q band frequencies provide compelling evidence for the presence of S=2 states, stable in a wide range of temperatures up to room temperature. A tentative model, corroborated by spin‐polarized...
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