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Bottom‐up electrochemical synthesis of atomically thin materials is desirable yet challenging, especially for non‐van der Waals (non‐vdW) materials. Thicknesses below a few nanometers have not been reported yet, posing the question how thin can non‐vdW materials be electrochemically synthesized. This is important as materials with (sub‐)unit‐cell thickness often show remarkably different properties...