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The optimal loading protocol of a microreactor (catalyst and inert: 0.1mm, column: 2mm internal diameter) with a catalyst–inert mixture is fundamentally different from that of a conventional lab-scale reactor (typical values: catalyst, 2mm; inert, 0.2mm; column, 10mm internal diameter). This is shown to be due to segregation, occurring during loading. The following loading procedure has been used:...
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