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A reusable heterogeneous catalytic assembly of [PO4{WO(O2)2}4]3− held in an ionic liquid brush was synthesized and an environmentally friendly procedure was developed for the dihydroxylation of several olefins with 30 wt% H2O2. These reactions were conducted in neat water under mild conditions without any organic co‐solvent or other additive. Several factors that affect the dihydroxylation were investigated...
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