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IR spectroscopic measurements have been used to chart the matrix photochemistry of ethyltrioxorhenium(VII). Broad-band UV–visible light (200≤λ≤800nm) results in the migration of a β-hydrogen atom of the ethyl group with the sequential formation of two tautomers, the first a weakly OH-bound ethene complex, C 2 H 4 ·HOReO 2 , and the second the η 2 -coordinated ethene...
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