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The design of soft biomaterials requires a deep understanding of molecular self‐assembly. Here a nanoscale infrared (IR) spectroscopy study of a two‐component supramolecular gel is introduced to assess the system's heterogeneity and supramolecular assembly. In contrast to far‐field IR spectroscopy, near‐field IR spectroscopy revealed differences in the secondary structures of the gelator molecules...
Circular dichroism (CD) spectroscopy has been used extensively for the investigation of the conformation and configuration of chiral molecules, but its use for evaluating the mode of self‐assembly in soft materials has been limited. Herein, we report a protocol for the study of such materials by electronic CD spectroscopy using commercial/benchtop instruments and synchrotron radiation (SR) using the...
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