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In this work X-ray single crystal structural analysis was carried out on the clathrate hydrate of tetraisoamylammonium propionate with the composition (i-C5H11)4NC2H5CO2·36H2O. The hydrate was found to have an orthorhombic structure in space group Cmc21 with unit cell parameters: a = 21.281(2) Å, b= 12.010(7) Å, c = 24.768(3) Å (150 K). X-ray powder diffraction studies were performed of the hydrate...