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The first dibromoalumanyl‐iron complex [Br2Al–FeCp(CO)2] was synthesized by the reaction of monobromoalumanyl‐iron complex bearing a bulky substituent on aluminum atom with AlBr3, whose structure was determined by the X‐ray crystallographic analysis and the NMR measurement. The reactions monobromoalumanyl‐iron complex with GaBr3 show that these reactions would proceed by the mutual recombination of...
Iron complex‐catalyzed dehydrogenative Sn–E (E = S, Se) bond formation of hydrostannane with thiol and selenol was achieved. All new compounds were fully characterized using 1H, 13C{1H}, 77Se{1H}, and 119Sn{1H} NMR measurements and elemental analyses. The structure of 1,1′‐(1,3‐dithia‐2,2‐dibutylstanyl)‐[3]ferrocenophane was confirmed by single‐crystal X‐ray diffraction.
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