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Rh(III)‐Catalyzed distal ortho‐C−H alkenylation of arylacetamides have been reported employing acetamide, a weak coordinating group, as a directing group. This challenging C−H alkenylation of arylacetamides has been achieved by using arylalkynyl silanes as a surrogate for terminal alkynes under redox neutral process through desilylation pathway. The control experiments suggest that the in situ generatedRh‐species...
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