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The tetradentate ligand 1,8-bis(2′-pyridyl)-3,6-dithiaoctane (Pdto) forms a pseudooctahedral structure with rhodium(III). The yellow racemic [Rh(Pdto)Cl2](CF3SO3) compound belongs to the Pbca space group with a = 13.566(15), b = 15.6588(16), c = 21.473(2) Å, and Z = 8. The Rh–S bonds are shorter than is usual, while the pyridine rings are mutually trans and form an interplanar angle of 24°. Graphical...
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