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Mixed-mode HPLC (MM-HPLC), combining different interactions or retention modes in a single column, can be an interesting alternative to reversed-phase HPLC, notably to achieve the combined retention of polar and non-polar species. In the present fundamental study, we have selected one bimodal stationary phase allowing for both reversed-phase and weak cation-exchange retention modes (Acclaim mixed-mode...
In this paper, a thioether-embedded mixed-mode cyano-bonded chromatographic packing has been prepared by using gas silylation method and thiol-ene click chemistry. The solid-state 13C CP/MAS NMR and elemental analysis have been used to characterize the synthesized materials. Detailed chromatographic characterization of the new phase was performed by alkyl benzene homologues in reversed-phase liquid...
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