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Fundamental material interactions as pertinent to nano-scale copper interconnects were studied for CVD Co with a variety of micro-analytical techniques. Native Co oxide grew rapidly within a few hours (XPS). Incorporation of oxygen and carbon in the CVD Co films (by AES and SIMS) depended on underlying materials, such as Ta, TaN, or Ru. Copper film texture (by XRD) and agglomeration resistance (by...
We have investigated electromigration process at metal nanojunctions as small as several tens of atoms and found that the elementary process of electromigration in such nanojunctions is the self-diffusion of metal atoms driven by microscopic kinetic energy transfer from single conduction electrons to single metal atoms. We have also shown that metal nanojunctions are stable and can support extremely...
A multilevel back-end-of-line structure with a dielectric constant κ ≤ 2.4 ultra low-κ materials was developed. κ=2.2 ULK build was demonstrated at a 144nm wiring pitch and a κ=2.4 ULK was demonstrated at a 288nm pitch. Good model-to-hardware correlation for the measured capacitance indicated no significant plasma damage to the ULK 2.2 material. The extracted copper resistivity was consistent with...
Downstream electromigration (EM) study was performed to investigate the cap layer and the grain size effects on Cu EM reliability for the 45 nm technology node. Four sets of Cu interconnects were examined: large and small grains with and without a CoWP cap placed between the SiCN cap and the Cu lines. Without the CoWP cap, the EM lifetime was reduced by a factor of 1.9 when changing from large to...
As the current-carrying capability of a copper line is reduced due to interconnect dimension shrinkage, self-aligned CoWP metal-cap has been reported to be helpful to improve degraded electromigration (EM) reliability. However, adoption of this new metal cap in general further exacerbates the already problematic low-k dielectric TDDB reliability at 32nm and beyond. This paper provides a comparative...
We have studied key factors of Ti-based self-formed barrier technique on interconnect reliability. A performance of time dependent dielectric breakdown shows superior endurance, using quite a thin Ti-based self-formed barrier. However, to achieve a superior electromigration performance using Ti-based self-formed barrier, much more amount of Ti is needed compared with that of TDDB performance. This...
A trade-off property of CuSiN between EM improvement and line resistance increase was resolved by a breakthrough that leaves oxygen at grain boundary of Cu line surface before CuSiN formation. Then, the combination of CuSiN and Ti-rich TiN (Ti(N)) barrier metal (-BM) was applied. Oxygen left by weakening process strength of CuOx reduction lowered line resistance, because Si diffusion causing line...
A Ti/TaN multi-layer can achieve a highly reliable Cu interconnect with a porous SiOC (ELK; k <; 2.5) structure. Ti shows good wettability with Cu and unique properties with extreme low-k (ELK)-structured interconnects. On the other hand, Ta is known to be an effective barrier to Cu diffusion. We confirmed that the Ti barrier is different from the Ta barrier from the viewpoint of metal-oxide behavior...
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