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A sensitive, rapid and efficient method for the extraction of quercetin as well as its determination in honey and biological samples was developed using inverted dispersive liquid–liquid microextraction (IDLLME) and HPLC-UV. The extraction method is based on the application of an extracting solvent lighter than water in the ternary component solvent (aqueous solution: extracting solvent: disperser...
A rapid and efficient capillary zone electrophoresis (CZE) method with ultraviolet detection has been successfully developed for the determination of puerarin in Xinkeshu capsules and biological samples. The optimal CZE conditions were determined to be 70mM H 3 BO 3 –Na 2 B 4 O 7 , pH 9.2, injection time 5s, applied voltage 25kV, working temperature 25°C and...
Two new ion-selective electrodes of the plastic membrane type for the determination of Tolterodine (Tol) were prepared. These electrodes depend on the incorporation of the ion-exchangers of the above mentioned drug with phosphotungestic acid (PTA) or Silicotungestic acid (STA) in a PVC matrix. A comparative study is made between the performance characteristics of electrodes containing ion-exchanger...
An automated, simple and inexpensive double-valve sequential injection analysis (DV-SIA) spectrophotometic method with online liquid–liquid extraction, for the determination of thiocyanate has been developed. The method has been based on the formation of an ion associate between thiocyanate and Astra Phloxine in acidic medium, and the subsequent extraction with amylacetate. The absorbance of the extracted...
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