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A new lead barium borate Ba8.02Pb0.98(B3O6)6 with B3O6 plane hexagonal rings was synthesized through spontaneous nucleation from a high-temperature solution utilizing PbO, H3BO3, and BaF2 as reagents. Its crystal structure was determined from single-crystal X-ray diffraction data and further characterized by FT-IR. It crystallizes in space group R32 and the crystallographic structure of Ba8.02Pb0.98...
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