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A large-scale purification procedure has been developed to isolate the membrane-bound bc 1 complex of Paracoccus denitrificans. From the purified complex, a water-soluble fragment has been isolated. The fragment comprising residues 50-190 contains the Rieske [2Fe-2S] cluster and has an optical spectrum which is typical of such a cluster. The EPR spectrum of the cluster in the bc 1 ...
The [Fe(C 7 H 7 N 4 S) 2 ]X·ηH 2 O (X = Cl (1), ClO 4 (2), NO 3 (3), PF 6 (4); n = 0 (4), 1.5 (1), 0.5 (3)) compounds, where C 7 H 8 N 4 S is pyridine-2-carbaldehyde thiosemicarbazone, have been synthesized and characterized. The crystal structure of compound 4 has been solved. It crystallizes in the monoclinic...
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