Syntheses, Crystal Structures, and Density Functional Theory Calculations of the c loso -[1-M(CO) 3 (η 4 -E 9 )] 4 - (E = Sn, Pb; M = Mo, W) Cluster Anions and Solution NMR Spectroscopic Characterization of [1-M(CO) 3 (η 4 -Sn 9 )] 4 - (M = Cr, Mo, W) †