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Studies of phosphorus cycling in the ocean have been greatly facilitated by the use of high molar activity 32P- and 33P-labeled phosphate (phosphoric acid) in biological incubation assays. Recently, phosphite (phosphorous acid) has been shown to play an important role in the ocean. Here I report the microscale (100 μmol) synthesis of high molar activity 33P-labeled phosphorous acid. The scheme incorporates...
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