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Cycloamylose containing 26 glucose residues (cyclohexaicosaose, CA26) crystallized from water and 30% (v/v) polyethyleneglycol 400 in the orthorhombic space group P2 1 2 1 2 1 in the highly hydrated form CA26.32.59 H 2 O. X-ray analysis of the crystals at 0.85 Å resolution shows that the macrocycle of CA26 is folded into two short left-handed V-amylose helices in antiparallel...
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