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Cyclic ADP-ribose mobilizes intracellular Ca2+ in a variety of cells. To elucidate the nature of the interaction between the C3′ substituent of cADP-ribose and the cADPR receptor, three analogues of NAD+ modified in the adenosine ribase (xyloNAD+ 3′F-xyloNAD+ and 3′F-NAD+ were chemically synthesised from d-xylose and adenine starting materials. 3′F-NAD+ was readily converted to cyclic 3′F-ADP ribose...
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