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The spatially separated bilayers of polypyrrole (PPy) doped with anions of limited (dodecylsulfate (DDS) and sulfate) and good mobility (chloride) have been prepared by consecutive electrodeposition. The perfect coverage of PPy in the inner layer was obtained already at a very low effective thickness (<0.05 μm) of the outer layer. The peculiarity of the redox behavior of PPy bilayers has been investigated...
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