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A planar network consisting of {Mo17(NO)2}3{MoV2}3{Fe 6III } cluster entities that are interlinked to layers via {FeII(H2O)4}2+ groups is formed stepwise from building units. The corresponding mixed-valence compound exhibits a variety of different formal oxidation states: {MoNO}3+, MoV, MoVI, FeII, and FeIII. This compound also represents an extension of building-block hierarchy from the molecular...
The compound [Mo 72 Fe 30 O 252 (CH 3 COO) 10 {Mo 2 O 7 (H 2 O)}{H 2 Mo 2 O 8 (H 2 O)} 3 (H 2 O) 91 ].ca. 140 H 2 O 3=3a.ca. 140 H 2 O, an important educt for an unusual solid state reaction, can now be obtained easily by reacting (NH...
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