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The relative electroactivities of different nickel surface structures, polycrystalline and (100), (111) and (210) planes, towards the hypophosphite ion oxidation are evaluated under carefully selected conditions to avoid both the electrode surface oxidation and background electrolyte competitive adsorption.Voltammetric and chronoamperometric studies have shown the hypophosphite ion oxidation dependence...
The Probe Beam Deflection (PBD) together with cyclic voltammetry and chronoamperometry have been used to study in-situ an electrocatalytic reaction: the hypophosphite ion electro-oxidation on the nickel electrode in the alkaline medium. The results are discussed in terms of a previously proposed mechanism and are consistent with the involvement of a non faradaic rate determining reaction preceding...
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