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We report the synthesis, crystallization, and solid‐state characterization of the 3,7‐ethoxy‐substituted spirobiphenalenyl‐boron neutral radical 22. The radical is distinguished by its low disproportionation energy and one‐dimensional structure. We show that our strategy of substitution of OEt group at the active positions of the phenalenyl units changes the crystal packing from its previously known...
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