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The structures in the solid state and solution state of tertiary group 15 ligand disubstituted derivatives of the heteronuclear cluster RuOs 3 (μ-H) 2 (CO) 13 are examined. Four structural types have been characterised crystallographically, including one in which both phosphine ligands were substituted at the unique ruthenium vertex. In solution, there are many more isomers...
The reaction of 1,1'-bis(diphenylphosphino)ferrocene (dppf) with a mixture of [MnRe(CO) 10 ], MeOH and Me 3 NO afforded the complexes fac-[MnH(CO) 3 (η 2 -dppf)] and [Re 2 (μ-OMe) 2 (μ-dppf)(CO) 6 ]. In the one-pot reaction of [Re 2 (CO) 10 ] with Me 3 NO, MeOH and dppf, the major mononuclear Re species isolated...
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