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In this work, we investigated the systems of (Li, Ca)–O–(Cl, Br) under high pressure and temperature for the synthesis of lithium-rich anti-perovskite (LiRAP) halides. We successfully synthesized Li3−xCax/2OCl anti-perovskite with x=0.0, 0.1, 0.2 near 0.5GPa and temperatures of 400–425K and Li3OBr anti-perovskite at 3.0GPa and 450K. Different from the synthetic route previously reported at ambient...
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