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The ceramics with the formula of Sr1−xSm2x/3TiO3 (x = 0‐0.5) were prepared by conventional ceramic process. A single phase of SrTiO3‐type with cubic perovskite structure was found companied with a decrease in crystal volume when x < 0.5, which was confirmed by X‐ray diffraction results and Rietveld refine. At the level of x = 0.5, the sample consisted of two phases of SrTiO3‐type and Sm2Ti2O7....