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Three‐dimensional porous platinum (Ptpor) films are prepared based on Pt electrodeposition on polyaniline (PANI) modified electrodes followed by selective dissolution of PANI with HNO3. Electrochemical quartz crystal microbalance data suggest that the PANI‐H2PtCl6 interaction involves redox and coordination reactions, depending on the working potential. The Ptpor shows better electrocatalytic performance...
Thionine (TH) adsorbed on multiwalled carbon nanotubes (MWCNTs) increases the load and dispersion of platinum nanoparticles (PtNPs) generated by chemical reduction of H2PtCl6 with NaBH4. Under the optimum conditions, the PtNPs‐TH‐MWCNTs/Au electrode electrocatalyzed the reduction and oxidation of H2O2 with high sensitivity, and after glucose oxidase (GOx) adsorption it responded to glucose concentration...
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