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Suzuki–Miyaura cross coupling reaction was used for access to new macrocycles exhibiting oligoethyleneoxide bridges and embedding bithiophene, terthiophene or 3,7-bis(thiophen-2-yl)-N-ethyl-10H-phenothiazine units. The synthesis was performed under various reaction conditions and different coupling types in order to establish the correlation between yields and employed solvents and bases. The structure...
The synthesis of monomers and dimers of some new crown ether type macrocycles with 1,4-phenylene and 1,4-naphthylene units are reported. The structural investigations of the compounds were carried out by NMR spectra, MS measurements and the single crystal X-ray solid state molecular structure of one compound.
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