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Chronoamperometry is carried out with a spherical Au electrode fused at the tip of a glass tube. The slope and intercept of the linear region of the current versus reciprocal square root of time are used to deduce the diffusion coefficient (D) without the need for the concentration of BH4- and the electron number involved in the oxidation of the anion. The D (in cm 2 s −1 ) of BH4-...
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